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ROMANA 3: a phase 3 safety extension study of anamorelin in advanced non-small cell lung cancer (NSCLC) patients with cachexia

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Cell 80 , 592606.e598 (2020)

Step 2 The product of step 1 (41.0 g) and KOH (32.0 g) was dissolved in 200 ml of methanol, added 35.5 ml bromoethane, heated under reflux for 2 h, added 200 ml of 5% NaOH after cooled, and reacted for 34 h, added 600 ml ice water after reaction, stirred, rested and filtered, washed with water, recrystallised with 500 ml ethanol and dried at 80 C